aReaction conditions: 1a (0.3 mmol) and
2a (0.9 mmol) at 100 °C for 5 h under air. Corrected GC yields
using n-dodecane as an internal standard were reported. n.d. =
not detected. b1a/2a = 1:1.
c1a/2a = 1:2. dUnder argon.
eIn dark. |
aReaction conditions:
1a (0.3 mmol) and 2a (0.9 mmol) at 100 °C for 5 h
under air. Corrected GC yields using n-dodecane as an internal
standard were reported. n.d. = not detected.
b1a/2a = 1:1.
c1a/2a = 1:2. dUnder argon.
eIn dark. |
aReaction conditions:
1a (0.3 mmol) and 2a (0.9 mmol) at 100 °C for 5 h
under air. Corrected GC yields using n-dodecane as an internal
standard were reported. n.d. = not detected.
b1a/2a = 1:1.
c1a/2a = 1:2. dUnder argon.
eIn dark. |
aReaction conditions:
1a (0.3 mmol) and 2a (0.9 mmol) at 100 °C for 5 h
under air. Corrected GC yields using n-dodecane as an internal
standard were reported. n.d. = not detected.
b1a/2a = 1:1.
c1a/2a = 1:2. dUnder argon.
eIn dark. |
aReaction conditions:
1a (0.3 mmol) and 2a (0.9 mmol) at 100 °C for 5 h
under air. Corrected GC yields using n-dodecane as an internal
standard were reported. n.d. = not detected.
b1a/2a = 1:1.
c1a/2a = 1:2. dUnder argon.
eIn dark. |
aReaction conditions:
1a (0.3 mmol) and 2a (0.9 mmol) at 100 °C for 5 h
under air. Corrected GC yields using n-dodecane as an internal
standard were reported. n.d. = not detected.
b1a/2a = 1:1.
c1a/2a = 1:2. dUnder argon.
eIn dark. |